Particle Size Characterization of an Extra Fine Milled Product

The present research aims to characterize the particle size distribution of sub micron particles suspended in a liquid. The particles milled are an organic poorly water soluble crystalline product. To characterize the size of these particles, different techniques have been tested: imaging techniques (SEM, CryoTEM), static light scattering techniques, dynamic light scattering techniques, centrifugation and flow field flow fractionation. The results indicate that the studied milled particles have a primary particle size close to 180nm and there is strong evidence of larger particles which are very likely aggregates. This is clearly seen from the Cryo TEM results. All the above mentioned techniques should in principle be able to measure samples of dispersion containing particles of ca 180 nm but several are disturbed by the presence of large aggregates. It is difficult to estimate the amount of aggregate present, but most of the time one is interested in what the primary particle size distribution is. It is clear that no single piece of equipment is capable of exactly determining the particle size distribution of our samples, but the static light scattering with low shear on mixing does give a good representation of what is seen with the image analysis by cryo TEM.     

基于分数阶傅立叶变换的线性调频回波参数估计

本文提出了一种适用于宽带线性调频回波的分数阶傅立叶变换参数估计方法。它通过寻找合适的信号代替发射信号做模版,使得模版信号与接收信号的模糊函数匹配度高,峰值尖锐,失真率低。再利用分数阶傅立叶变换与模糊函数的关系,使用两次分数阶域的峰值搜索代替原有的一次二维搜索降低计算量。仿真实验结果表明,本文提出的方法在精确估计宽带回波的时延和频移的同时降低了计算复杂度。     

水声换能器研究新进展

文章综述了几种典型结构水声换能器近些年的新发展,包括:弯张换能器、圆柱面辐射型换能器、纵向换能器等等,主要介绍这些结构类型水声换能器的设计新思想和多方面优化改进的新成果。     

气体声弛豫过程中有效比热容与弛豫时间的分解对应关系

声在多原子分子气体中传播所引起的弛豫过程是探索气体特性的重要方面. 本文通过研究气体声弛豫过程中振动自由度与平动自由度(V-T)以及振动自由度之间(V-V)的分子能量转移模型, 给出了有效比热容与弛豫时间的分解对应关系及其通用获得方法. 该分解模型与现有的声弛豫模型相比, 反映了分解后的V-T 和V-V弛豫过程中振动比热容与弛豫时间的对应关系, 并发现了较高能级是引起对应声弛豫过程的决定因素. 将基于该分解模型获得的气体声弛豫衰减谱经碰撞直径微调改进后, 比现有理论更接近实验数据, 其结果证明了该分解对应关系的正确性和合理性.     

水下强声波脉冲负压的产生和空化气泡运动

首先利用高速摄影和压力传感器测量的方法, 对曲面反射式水下强声波脉冲的传播和聚焦过程进行了实验研究.实验研究发现, 椭球面反射罩在起到汇聚声能的作用的同时也将使得强声波脉冲在传播过程中形成负压区, 并由此而引发近场声传播通道上空化气泡群的产生. 在实验结果的基础上, 进一步利用基于Kirchhoff衍射定理的声传播模型和大振幅条件下的QX气泡运动方程, 对强声波脉冲负压区的形成原因及空化气泡的运动过程进行了数值计算和分析. 研究结果表明, 在焦前区, 源于反射罩内表面的"尾波"和出口处的"边缘波"在传播过程中将形成反射波中的负压区; 在焦后区, 源于反射罩顶点的"中心波"在传播过程中将形成反射波中的负压区. 在反射波作用下, 空化气泡体现出了"正压区受压缩并振荡, 负压区膨胀"的运动特点. 在反射波之后, 空化气泡将出现成长、坍缩和回弹等典型的物理过程. 研究结果对曲面反射式水下强声波传播物理规律的认识具有实际意义.     

一维指数形变截面有限周期声子晶体的研究

本文利用集中质量法对弹性纵波在一维指数形截面有限周期声子晶体中的传播进行了研究, 得到了频率响应函数的表达式. 与一维等截面的声子晶体相比, 指数形变截面声子晶体带隙内的衰减值随着输出端截面积的增大而减小, 同时带隙的起始频率降低而截止频率升高, 也即带隙的宽度会得到拓展. 晶格常数和材料组份比变化时, 变截面声子晶体带隙的起始频率和截止频率的变化趋势与等截面时的声子晶体相同. 希望本文的研究能够推动声子晶体在减振降噪等领域中的应用.     

立体图像质量的主观评价方案

立体图像质量评价在立体图像压缩、处理以及通信领域中有着十分重要的作用,一种好的立体图像质量客观评价方法也要依赖于立体图像的主观评价.本文基于人眼的立体视觉特性,提出了相对完整的立体图像质量主观评价方案,该方案主要分为立体图像库的建立、评测者的选择、观看条件的描述、评测者的训练和测试、数据处理和实验结果分析六个方面.实验中,评测者根据自己的主观感受,对所选取的立体图像进行评分,最后用数理统计理论对所得数据进行处理.结果表明,本文所提出的主观评价方案可行,能够正确反映立体图像质量的优劣.     

Intrinsic anisotropy of the effective acoustic properties in metafluids made of two-dimensional cylinder arrays

Within a unified theoretical framework, we extract the omnidirectional effective acoustic parameters for the metafluid consisting of isotropic fluid cylinders embedded in an isotropic fluid background. Besides the analytical formulas for the effective parameters reported previously, i.e., the bulk modulus and the mass density perpendicular to the cylinders, we also derive a simple expression for the effective mass density parallel to the cylinders. As expected, these two effective mass densities are not identical and constitute an anisotropic density tensor. Such intrinsic anisotropy can be engineered much stronger than the pure in-plane anisotropy induced by either anisotropic lattices or anisotropic scatterers.     

基于LabVIEW激光引信回波模拟装置设计

激光引信回波模拟装置是激光引信测试设备的重要组成部分。介绍了激光引信回波模拟装置的组成,设计了用于该装置的硬件电路和软件控制系统。硬件电路采用单片机完成控制指令的接收和控制信号的产生,使用串行扩展芯片GM8125将单片机AT89S52的串行口扩展成5个,满足了激光引信回波模拟装置串口资源要求。软件控制系统基于LabVlFⅣ设计,主要包括串口通信程序和控制指令的产生程序,控制指令经串口通信传送给硬件电路。实验结果表明,该装置满足激光引信测试设备的要求。     

Tunable Ba0.5Sr0.5TiO3 film bulk acoustic resonators using SiO2/Mo Bragg reflectors

Tunable and switchable Ba 0.5 Sr 0.5 TiO 3 film bulk acoustic resonators（FBARs） based on SiO 2 /Mo Bragg reflectors are explored,which can withstand high temperature for the deposition of Ba x Sr 1 x TiO 3（BST） films at 800 C.The dc bias-dependent resonance may be attributed to the piezoelectricity of the BST film induced by an electrostrictive effect.The series resonant frequency is strongly dc bias-dependent and shifts downwards with dc bias increasing,while the parallel resonant frequency is only weakly dc bias-dependent and slightly shifts upwards at low dc bias（ 45 V） while downwards at higher dc bias.The calculated relative tunability of shifts at series resonance frequency is around 2.3% and the electromechanical coupling coefficient is up to approximately 8.09% at 60-V dc bias,which can be comparable to AlN FBARs.This suggests that a high-quality tunable BST FBAR device can be achieved through the use of molybdenum（Mo） as the high acoustic impedance layer in a Bragg reflector,which not only provides excellent acoustic isolation from the substrate,but also improves the crystallinity of BST films withstanding higher deposition temperature.